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The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance

Powder Metallurgy (PM) offers an advantageous route for manufacturing complex and near net-shape components. Their inherent interconnected porosity that promotes the action of self lubrication compromises their structural integrity by creating pathways for corrosion and excessive wear. This research...

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Main Author: Abdelfadeel, Maha Khaled
Format: Thesis
Published: AUC Knowledge Fountain 2026
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access_status_str Open Access
author Abdelfadeel, Maha Khaled
author_browse Abdelfadeel, Maha Khaled
author_facet Abdelfadeel, Maha Khaled
author_sort Abdelfadeel, Maha Khaled
collection Thesis
description Powder Metallurgy (PM) offers an advantageous route for manufacturing complex and near net-shape components. Their inherent interconnected porosity that promotes the action of self lubrication compromises their structural integrity by creating pathways for corrosion and excessive wear. This research investigates the efficacy of Multi-Walled Carbon Nanotubes (MWCNTs) as a nano additive within the impregnating base oil (SN-150 base oil). An experimental matrix was designed to evaluate the influence of MWCNTs with different concentrations of 0.05, 0.1, and 0.2 wt.% and ultrasonic dispersion with varying sonication times of 30 and 60 minutes on the tribological and electrochemical performance of sintered steel self-lubricating bushings. The study confirms that the use of MWCNTs -based nanofluids can successfully penetrate the porous sintered steel structures, achieving oil content exceeding 19% across all specimens. In tribological performances, lower concentrations of MWCNTs proved superior, where specimens impregnated with nanofluid (NF) containing 0.05 wt.% MWCNTs, sonicated for 60 minutes, exhibited approximately 90% reduction in wear rate, resulting in a value of 0.45mg/km compared to reference specimen achieving 4.7mg/km, and a stabilized coefficient of friction, induced by the rolling-effect mechanism of the dispersed MWCNTs. On the other hand, electrochemical polarization test method revealed that with increasing MWCNTs concentrations, corrosion resistance increases. NF, containing 0.2 wt.% MWCNTs, and sonicated for 60 minutes, exhibited an inhibition efficiency of approximately 82% and reduced the corrosion rate to 0.18 mm/year, compared to the reference specimen which demonstrated 1.02 mm/year. The resulting findings establish MWCNTs-NF as an impregnation lubricant a transformative approach for PM components, optimizing their mechanical properties and environmental resistance to meet industrial application requirements.
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id oai:fount.aucegypt.edu:etds-3795
institution American University in Cairo (Egypt)
last_indexed 2026-06-10T12:36:04.472Z
license_str Not specified — see source repository
provenance_str_mv Harvested via OAI-PMH from AUC Knowledge Fountain — bepress
publishDate 2026
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spelling oai:fount.aucegypt.edu:etds-3795 The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance Abdelfadeel, Maha Khaled Powder Metallurgy (PM) offers an advantageous route for manufacturing complex and near net-shape components. Their inherent interconnected porosity that promotes the action of self lubrication compromises their structural integrity by creating pathways for corrosion and excessive wear. This research investigates the efficacy of Multi-Walled Carbon Nanotubes (MWCNTs) as a nano additive within the impregnating base oil (SN-150 base oil). An experimental matrix was designed to evaluate the influence of MWCNTs with different concentrations of 0.05, 0.1, and 0.2 wt.% and ultrasonic dispersion with varying sonication times of 30 and 60 minutes on the tribological and electrochemical performance of sintered steel self-lubricating bushings. The study confirms that the use of MWCNTs -based nanofluids can successfully penetrate the porous sintered steel structures, achieving oil content exceeding 19% across all specimens. In tribological performances, lower concentrations of MWCNTs proved superior, where specimens impregnated with nanofluid (NF) containing 0.05 wt.% MWCNTs, sonicated for 60 minutes, exhibited approximately 90% reduction in wear rate, resulting in a value of 0.45mg/km compared to reference specimen achieving 4.7mg/km, and a stabilized coefficient of friction, induced by the rolling-effect mechanism of the dispersed MWCNTs. On the other hand, electrochemical polarization test method revealed that with increasing MWCNTs concentrations, corrosion resistance increases. NF, containing 0.2 wt.% MWCNTs, and sonicated for 60 minutes, exhibited an inhibition efficiency of approximately 82% and reduced the corrosion rate to 0.18 mm/year, compared to the reference specimen which demonstrated 1.02 mm/year. The resulting findings establish MWCNTs-NF as an impregnation lubricant a transformative approach for PM components, optimizing their mechanical properties and environmental resistance to meet industrial application requirements. 2026-06-15T07:00:00Z thesis application/pdf https://fount.aucegypt.edu/etds/2736 https://fount.aucegypt.edu/context/etds/article/3795/viewcontent/Maha_Khaled_Abdelfadeel_Thesis.pdf Theses and Dissertations AUC Knowledge Fountain MWCNTs Powder Metallurgy Oil impregnation Nanofluids Sintered Steel Engineering Manufacturing Materials Science and Engineering Mechanical Engineering Metallurgy Tribology
spellingShingle MWCNTs
Powder Metallurgy
Oil impregnation
Nanofluids
Sintered Steel
Engineering
Manufacturing
Materials Science and Engineering
Mechanical Engineering
Metallurgy
Tribology
Abdelfadeel, Maha Khaled
The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance
title The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance
title_full The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance
title_fullStr The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance
title_full_unstemmed The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance
title_short The Effect of MWCNT-Oil Impregnation of Sintered Components on Their Wear and Corrosion Resistance
title_sort effect of mwcnt oil impregnation of sintered components on their wear and corrosion resistance
topic MWCNTs
Powder Metallurgy
Oil impregnation
Nanofluids
Sintered Steel
Engineering
Manufacturing
Materials Science and Engineering
Mechanical Engineering
Metallurgy
Tribology
url https://fount.aucegypt.edu/etds/2736
https://fount.aucegypt.edu/context/etds/article/3795/viewcontent/Maha_Khaled_Abdelfadeel_Thesis.pdf
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