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A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite

This work concerned the design and development of a miniature double torsion (DT) testing rig, for use inside the chamber of a scanning electron microscope, to perform in situ loading studies of brittle materials using the DT fracture mechanics specimen. The in situ performance of the system inside...

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Main Author: Rosie, Kathryn A
Format: Thesis
Language:English
Published: Department of Mechanical Engineering 2015
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access_status_str Open Access
author Rosie, Kathryn A
author_browse Rosie, Kathryn A
author_facet Rosie, Kathryn A
author_sort Rosie, Kathryn A
collection Thesis
description This work concerned the design and development of a miniature double torsion (DT) testing rig, for use inside the chamber of a scanning electron microscope, to perform in situ loading studies of brittle materials using the DT fracture mechanics specimen. The in situ performance of the system inside the SEM was highly satisfactory, while still providing free rotation of the attached stepper motor. Crack growth rates of down to 19nm/s were directly observed in PMMA specimens. It was concluded that the technique displayed merit in its ability to contribute to the knowledge base of slow cracking and damage development in brittle materials, with the advantage being that the gearing ratios of the current device resulted in slower specimen loading rates, which were more controlled, than reported previously.
format Thesis
id oai:open.uct.ac.za:11427/11099
institution University of Cape Town (South Africa)
language eng
last_indexed 2026-06-10T12:45:12.212Z
license_str Not specified — see source repository
provenance_str_mv Harvested via OAI-PMH from UCTD — University of Cape Town Open Access Repository
publishDate 2015
publishDateRange 2015
publishDateSort 2015
publisher Department of Mechanical Engineering
publisherStr Department of Mechanical Engineering
record_format dspace
source_str UCTD — University of Cape Town Open Access Repository
spelling oai:open.uct.ac.za:11427/11099 A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite Rosie, Kathryn A Mechanical Engineering This work concerned the design and development of a miniature double torsion (DT) testing rig, for use inside the chamber of a scanning electron microscope, to perform in situ loading studies of brittle materials using the DT fracture mechanics specimen. The in situ performance of the system inside the SEM was highly satisfactory, while still providing free rotation of the attached stepper motor. Crack growth rates of down to 19nm/s were directly observed in PMMA specimens. It was concluded that the technique displayed merit in its ability to contribute to the knowledge base of slow cracking and damage development in brittle materials, with the advantage being that the gearing ratios of the current device resulted in slower specimen loading rates, which were more controlled, than reported previously. 2015-01-03T05:33:29Z 2015-01-03T05:33:29Z 2011 Master Thesis Masters MSc http://hdl.handle.net/11427/11099 eng application/pdf Department of Mechanical Engineering Faculty of Engineering and the Built Environment University of Cape Town
spellingShingle Mechanical Engineering
Rosie, Kathryn A
A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite
thesis_degree_str Master's
title A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite
title_full A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite
title_fullStr A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite
title_full_unstemmed A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite
title_short A method for in situ SEM fracture studies of brittle materials using the double torsion technique : application to nuclear graphite
title_sort method for in situ sem fracture studies of brittle materials using the double torsion technique application to nuclear graphite
topic Mechanical Engineering
url http://hdl.handle.net/11427/11099
work_keys_str_mv AT rosiekathryna amethodforinsitusemfracturestudiesofbrittlematerialsusingthedoubletorsiontechniqueapplicationtonucleargraphite
AT rosiekathryna methodforinsitusemfracturestudiesofbrittlematerialsusingthedoubletorsiontechniqueapplicationtonucleargraphite