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Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction

Resistance thermometers are often made of thin, sputter-deposited platinum layers on a corundum substrate. Since such thermometers are usually exposed to extreme temperatures, residual stress is building up at the Pt-Ah03 interface and can possibly damage the layer. Therefore, the stress in the laye...

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Main Author: Bollhofer, Axel
Other Authors: Härting, Margit
Format: Thesis
Language:English
Published: Department of Physics 2023
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access_status_str Open Access
author Bollhofer, Axel
author2 Härting, Margit
author_browse Bollhofer, Axel
Härting, Margit
author_facet Härting, Margit
Bollhofer, Axel
author_sort Bollhofer, Axel
collection Thesis
description Resistance thermometers are often made of thin, sputter-deposited platinum layers on a corundum substrate. Since such thermometers are usually exposed to extreme temperatures, residual stress is building up at the Pt-Ah03 interface and can possibly damage the layer. Therefore, the stress in the layer is measured by means of non-destructive x-ray diffraction and evaluated by the frequently used "d-sin21/J" method. The apparatus for the measurements was a Q-goniometer with a Bragg-Brentano focusing beam arrangement and a position sensitive detector. X-ray fluorescence scans were also performed on the sample in order to gain information about its composition. Additionally, a scanning-electron-microscope was used to investigate its microstructure. The crystallographic texture of the platinum was also examined by x-ray diffraction and displayed in pole figures.
format Thesis
id oai:open.uct.ac.za:11427/38444
institution University of Cape Town (South Africa)
language eng
last_indexed 2026-06-10T12:33:54.099Z
license_str Not specified — see source repository
provenance_str_mv Harvested via OAI-PMH from UCTD — University of Cape Town Open Access Repository
publishDate 2023
publishDateRange 2023
publishDateSort 2023
publisher Department of Physics
publisherStr Department of Physics
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source_str UCTD — University of Cape Town Open Access Repository
spelling oai:open.uct.ac.za:11427/38444 Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction Bollhofer, Axel Härting, Margit Physics Resistance thermometers are often made of thin, sputter-deposited platinum layers on a corundum substrate. Since such thermometers are usually exposed to extreme temperatures, residual stress is building up at the Pt-Ah03 interface and can possibly damage the layer. Therefore, the stress in the layer is measured by means of non-destructive x-ray diffraction and evaluated by the frequently used "d-sin21/J" method. The apparatus for the measurements was a Q-goniometer with a Bragg-Brentano focusing beam arrangement and a position sensitive detector. X-ray fluorescence scans were also performed on the sample in order to gain information about its composition. Additionally, a scanning-electron-microscope was used to investigate its microstructure. The crystallographic texture of the platinum was also examined by x-ray diffraction and displayed in pole figures. 2023-09-07T11:18:44Z 2023-09-07T11:18:44Z 1999 2023-09-07T11:08:13Z Master Thesis Masters MSc http://hdl.handle.net/11427/38444 eng application/pdf Department of Physics Faculty of Science
spellingShingle Physics
Bollhofer, Axel
Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction
thesis_degree_str Master's
title Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction
title_full Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction
title_fullStr Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction
title_full_unstemmed Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction
title_short Study of residual stress in a thin platinum layer by means of nondestructive x-ray diffraction
title_sort study of residual stress in a thin platinum layer by means of nondestructive x ray diffraction
topic Physics
url http://hdl.handle.net/11427/38444
work_keys_str_mv AT bollhoferaxel studyofresidualstressinathinplatinumlayerbymeansofnondestructivexraydiffraction