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Experimental investigation and statistical analysis of pulp vacuum dewatering

Thesis (MEng)--Stellenbosch University, 2024.

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Main Author: Mafela, Mahlohonono Precious
Other Authors: Görgens, Johann Ferdinand
Format: Thesis
Language:en_ZA
Published: Stellenbosch : Stellenbosch University 2024
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access_status_str Open Access
author Mafela, Mahlohonono Precious
author2 Görgens, Johann Ferdinand
author_browse Görgens, Johann Ferdinand
Mafela, Mahlohonono Precious
author_facet Görgens, Johann Ferdinand
Mafela, Mahlohonono Precious
author_sort Mafela, Mahlohonono Precious
collection Thesis
dc_rights_str_mv Stellenbosch University
description Thesis (MEng)--Stellenbosch University, 2024.
format Thesis
id oai:scholar.sun.ac.za:10019.1/130524
institution Stellenbosch University (South Africa)
language en_ZA
last_indexed 2026-06-10T12:43:19.203Z
license_str Other — see source repository
provenance_str_mv Harvested via OAI-PMH from SUNScholar — Stellenbosch University Repository
publishDate 2024
publishDateRange 2024
publishDateSort 2024
publisher Stellenbosch : Stellenbosch University
publisherStr Stellenbosch : Stellenbosch University
record_format dspace
source_str SUNScholar — Stellenbosch University Repository
spelling oai:scholar.sun.ac.za:10019.1/130524 Experimental investigation and statistical analysis of pulp vacuum dewatering Mafela, Mahlohonono Precious Görgens, Johann Ferdinand Tyhoda, Luvuyo Louw, Tobias Muller Stellenbosch University. Faculty of Engineering. Dept. of Chemical Engineering. Process Engineering. Pulping -- South Africa Papermaking -- Chemistry -- South Africa Paper -- Dewatering -- South Africa Vacuum -- Industrial applications -- South Africa Thesis (MEng)--Stellenbosch University, 2024. ENGLISH ABSTRACT: Energy consumption in the forming section of a paper machine is high due to the process requirement for vacuum. Thus, making it imperative to explore various energy conservation opportunities in this early stage of water removal. Most of the vacuum generated is utilised in the high vacuum dewatering zone of the section to remove filtrate from pulp slurries at various durations or dwell times. Therefore, the effects of vacuum pressure and dwell time on the achievable solids content of pulp samples refined at different levels of energy were studied. A laboratory suction box was constructed to simulate pulsation effects experienced by pulp slurries in the forming section of paper machines during high vacuum dewatering. A rotating spindle with slots each with a length the same as the diameter of the sample holder was utilised to generate suction pulses at speeds as high as 400 m/min. A pressure profile was generated from data obtained during experimental investigation and compared to the pressure profile from the high vacuum zone of a paper machine. It was determined that the pulses generated by the setup adequately replicated the performance of suction boxes in industrial formers. The dynamic setup could generate suction pulses with a duration of only 6 ms. Three pulp types that each represent a unique pulping process in the South African pulp and paper industry were tested. These included bleached hardwood, mechanical or groundwood and pure K3 (New corrugated kraft waste) recycled pulp. Sample characterisation of the pulps was done before exposure to vacuum, to obtain pulp fibre morphology and analyse their water-fibre interactions, i.e., freeness and the water retention value. Statistical analysis of the fibre characterisation results through ANOVA and ANCOVA revealed that an increase in the refining energy appreciably affected freeness and water retention value. Pearson’s coefficients further revealed that refining had a positive relationship with the water retention value whereas the opposite was true for pulp freeness or drainability. ANCOVA of pulp morphology with respect to virgin pulp drainability and water retention showed that only the shape factor and fibre length was significant for bleached hardwood pulp’s water retention and freeness. For mechanical pulp, only fines content and fibre length affected drainability and water retention. High vacuum dewatering results of the characterised pulps revealed a dry matter/ concentration plateau for dwell times ranging from 30 to 135 ms. However, there was in increase in the dry matter of all pulp types at a dwell time of 250 ms. Diminishing returns exponential trendlines were fitted into the vacuum dewatering experimental data to better characterise and predict the pulp dry matter or concentration of the three pulps. The trendlines effectively showed the dewatering behaviour of pulp samples where a plateau in the predicted pulp concentration or dry matter was observed. This is especially true for dwell times ranging from 30 to 135 ms. Statistical analysis through ANOVA showed that vacuum pressure crucially affects pulp dry matter. However, the linear regression analysis method could not establish an effect of the dwell time on dry matter. This does not signify its absence as the relationship is exponential, making it difficult to analyse through linear means. Lower vacuum pressures were associated with drier pulps. ANCOVA proved that water retention value and freeness had a statistically significant relationship with dewatering rate and plateau pulp concentration of pulps. Pulps with high drainability and water retention capacity performed better during vacuum dewatering, namely bleached hardwood, and recycled pulp. AFRIKAANSE OPSOMMING: Geen opsomming beskikbaar. Masters 2024-03-05T09:33:25Z 2024-04-26T20:44:49Z 2024-03-05T09:33:25Z 2024-04-26T20:44:49Z 2024-03 Thesis https://scholar.sun.ac.za/handle/10019.1/130524 en_ZA Stellenbosch University 186 pages : illustrations application/pdf Stellenbosch : Stellenbosch University
spellingShingle Pulping -- South Africa
Papermaking -- Chemistry -- South Africa
Paper -- Dewatering -- South Africa
Vacuum -- Industrial applications -- South Africa
Mafela, Mahlohonono Precious
Experimental investigation and statistical analysis of pulp vacuum dewatering
title Experimental investigation and statistical analysis of pulp vacuum dewatering
title_full Experimental investigation and statistical analysis of pulp vacuum dewatering
title_fullStr Experimental investigation and statistical analysis of pulp vacuum dewatering
title_full_unstemmed Experimental investigation and statistical analysis of pulp vacuum dewatering
title_short Experimental investigation and statistical analysis of pulp vacuum dewatering
title_sort experimental investigation and statistical analysis of pulp vacuum dewatering
topic Pulping -- South Africa
Papermaking -- Chemistry -- South Africa
Paper -- Dewatering -- South Africa
Vacuum -- Industrial applications -- South Africa
url https://scholar.sun.ac.za/handle/10019.1/130524
work_keys_str_mv AT mafelamahlohononoprecious experimentalinvestigationandstatisticalanalysisofpulpvacuumdewatering