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Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes

Thesis (MIng)--University of Stellenbosch, 2000.

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Main Author: Koen, Louis Johannes
Other Authors: Sanderson, R. D.
Format: Thesis
Language:en_ZA
Published: Stellenbosch : Stellenbosch University 2015
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access_status_str Open Access
author Koen, Louis Johannes
author2 Sanderson, R. D.
author_browse Koen, Louis Johannes
Sanderson, R. D.
author_facet Sanderson, R. D.
Koen, Louis Johannes
author_sort Koen, Louis Johannes
collection Thesis
dc_rights_str_mv Stellenbosch University
description Thesis (MIng)--University of Stellenbosch, 2000.
format Thesis
id oai:scholar.sun.ac.za:10019.1/97524
institution Stellenbosch University (South Africa)
language en_ZA
last_indexed 2026-06-10T12:43:57.787Z
license_str Other — see source repository
provenance_str_mv Harvested via OAI-PMH from SUNScholar — Stellenbosch University Repository
publishDate 2015
publishDateRange 2015
publishDateSort 2015
publisher Stellenbosch : Stellenbosch University
publisherStr Stellenbosch : Stellenbosch University
record_format dspace
source_str SUNScholar — Stellenbosch University Repository
spelling oai:scholar.sun.ac.za:10019.1/97524 Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes Koen, Louis Johannes Sanderson, R. D. Lorenzen, L. Stellenbosch University. Faculty of Engineering. Dept. of Process Engineering. Liquid separation processes Fouling layer formation Plant operation Ultrasonic-time-domain-reflectometry (UTDR) Dissertations -- Chemical engineering Thesis (MIng)--University of Stellenbosch, 2000. ENGLISH ABSTRACT: Fouling is readily acknowledged as one of the most critical problems limiting the wider application of membranes in liquid separation processes. A better understanding of fouling layer formation and its monitoring is needed in order to improve on existing cleaning techniques. Plant operation can be optimised if fouling can be monitored by noninvasion means either on the plant itself or on an attached monitoring device. The overall scope of this research was to develop a non-destructive, real-time, in situ visualisation technique or device for concentration polarisation and fouling layer monitoring. Ultrasonic-time-domain-reflectometry (UTDR) was employed as a visualisation technique to provide real-time characterisation of the fouling layer. A 24 cm-long rectangular flat sheet aluminium cell was designed and used as separation device for a desalination system. The experimental results obtained using this module confirmed that there are an excellent correspondence between the flux decline behaviour and the UTDR response from the membrane. The ultrasonic technique could effectively detect fouling layer initiation and growth on the membrane in real-time. In addition to the measurement of fouling, the ultrasonic technique was also successfully employed for monitoring membrane cleaning. Since no real-time permeation data is available during cleaning operations in industrial applications, a UTDR monitoring device may prove to be a very valuable technique in optimising cleaning strategies. The technique was further tested on an 8-inch diameter spiral wrap industrial module and good results were obtained. Stagnant zones, as well as flux flow behaviour inside the module could be determined. However, more research IS needed to fully understand the complex phenomena inside a spiral wrap module. Overall, the UTDR technique and its use in monitoring devices have a major impact in the membrane industry due to its extremely powerful capabilities. AFRIKAANSE OPSOMMING: Membraan-bevuiling of -verstopping is die grootste struikelblok wat die algemene aanwending van membrane vir verskillende watersuiweringsprosesse negatief beinvloed. 'n Beter begrip van membraan-bevuiling, asook beter metingsmetodes daarvan is nodig om op bestaande skoonmaaktegnieke te verbeter. Die hoofdoel van hierdie studie was die ontwikkeling van 'n nie-destruktiewe-in-lyn visuele tegniek vir die meting van konsentrasie polarisasie en membraan-bevuiling. Deur gebruik te maak van ultrasoniese klank golwe, is 'n tegniek ontwikkel wat 'n direkte visuele aanduiding kon gee van die toestand van membraan-bevuiling binnein die module. 'n Reghoekige aluminium-module, 24 cm lank, is ontwerp en gebou waarbinne die membraan geplaas is vir die skeidingsproses. Resultate dui daarop dat daar 'n uitstekende verband bestaan tussen die afname in permeaatvloei en die ultrasoniese eggo vanaf die membraan. Die ultrasoniese tegniek kon die vorming van en toename in membraan-bevuiling doeltreffend karakteriseer. In teenstelling hiermee, is die tegniek ook suksesvol aangewend om die skoonmaak-proses van membrane te ondersoek. Met min of geen data beskikbaar vir die skoonmaak-proses van membrane in die industriële sektor, het die tegniek enorme potensiaal in die optimisering van bestaande skoonmaak-tegnieke. Die tegniek is verder aangewend op 'n industriële 8-duim deursnee spiraal-module en goeie resultate is verkry. Stagnante sones asook vloed-vloei-patrone binne-in die module kon suksesvol bepaal word. Baie navorsing is egter nog nodig om die ingewikkelde data wat gegenereer word tydens die ondersoek van 'n spiraal-module ten volle te verstaan. Die enorme potensiaal en moontlikhede van die ultrasoniese tegniek kan die begin wees van 'n revolusie in die membraan-industrie. 2015-10-01T13:41:44Z 2015-10-01T13:41:44Z 2000-12 Thesis http://hdl.handle.net/10019.1/97524 en_ZA Stellenbosch University application/pdf Stellenbosch : Stellenbosch University
spellingShingle Liquid separation processes
Fouling layer formation
Plant operation
Ultrasonic-time-domain-reflectometry (UTDR)
Dissertations -- Chemical engineering
Koen, Louis Johannes
Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
title Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
title_full Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
title_fullStr Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
title_full_unstemmed Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
title_short Ultrasonic-time-domain-reflectometry as a real time non-destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
title_sort ultrasonic time domain reflectometry as a real time non destructive visualisation technique of concentration polarisation and fouling on reverse osmosis membranes
topic Liquid separation processes
Fouling layer formation
Plant operation
Ultrasonic-time-domain-reflectometry (UTDR)
Dissertations -- Chemical engineering
url http://hdl.handle.net/10019.1/97524
work_keys_str_mv AT koenlouisjohannes ultrasonictimedomainreflectometryasarealtimenondestructivevisualisationtechniqueofconcentrationpolarisationandfoulingonreverseosmosismembranes