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Chemical, sensory and consumer analysis of cork taint in South African wines

Thesis (MSc Food Sc (Food Science))--University of Stellenbosch, 2009.

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Main Author: Van Eeden, Petrus Rabe
Other Authors: Muller, Nina
Format: Thesis
Language:English
Published: Stellenbosch : University of Stellenbosch 2009
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access_status_str Open Access
author Van Eeden, Petrus Rabe
author2 Muller, Nina
author_browse Muller, Nina
Van Eeden, Petrus Rabe
author_facet Muller, Nina
Van Eeden, Petrus Rabe
author_sort Van Eeden, Petrus Rabe
collection Thesis
dc_rights_str_mv University of Stellenbosch
description Thesis (MSc Food Sc (Food Science))--University of Stellenbosch, 2009.
format Thesis
id oai:scholar.sun.ac.za:10019.1/2092
institution Stellenbosch University (South Africa)
language English
last_indexed 2026-06-10T12:44:24.894Z
license_str Other — see source repository
provenance_str_mv Harvested via OAI-PMH from SUNScholar — Stellenbosch University Repository
publishDate 2009
publishDateRange 2009
publishDateSort 2009
publisher Stellenbosch : University of Stellenbosch
publisherStr Stellenbosch : University of Stellenbosch
record_format dspace
source_str SUNScholar — Stellenbosch University Repository
spelling oai:scholar.sun.ac.za:10019.1/2092 Chemical, sensory and consumer analysis of cork taint in South African wines Van Eeden, Petrus Rabe Muller, Nina Nieuwoudt, Helene Tredoux, Andreas Naes, Tormod Matforsk, Nofima University of Stellenbosch. Faculty of Agrisciences. Dept. of Food Science. Cork taint Dissertations -- Food science Theses -- Food science Bottle corks Wine -- Flavor and odor -- South Africa Wine tasting -- South Africa Thesis (MSc Food Sc (Food Science))--University of Stellenbosch, 2009. This study focused on a serious quality-related problem in the global wine industry, including the South African Wine Industry, namely cork taint in wine. Annually, large financial losses are incurred by cork suppliers and wine producers, as a result of cork-tainted wine. Although contaminated new unused corks are frequently implicated as the origin of this taint, contaminated cellar equipment and water can also be the source of the problem. An explorative investigation into the incidence of cork taint in South African wines showed that 3.8% of the 133 wines tested, contained 2,4,6-trichloroanisole (TCA) concentrations of 3.5 ng/L and higher, as determined by gas chromatography coupled with electron capture detection (GC-ECD). TCA concentrations higher than 1 ng/L were found in 18% of the wines tested. All affected wines were sealed with solid or agglomerate cork stoppers. These wines were sourced from various wineries in the Western Cape region, South Africa and were of different cultivars. None of the wines sealed with synthetic closures had any detectable TCA, 2,4,6-tribromoanisole (TBA) or pentachloroanisole (PCA) levels and only very low 2,3,4,6- tetrachloroanisole (TeCA) levels (1 ng/L or less). Another group of 28 wines that were rejected by the official South African wine regulatory body on the basis of the presence of mouldy taint during wine certification, was also included in this study. GC-ECD analysis showed that 30% of the wines in this group contained TCA at concentrations of 3.5 ng/L and higher. These results pointed to a relative high incidence of TCA in the wines investigated, especially those sealed with cork stoppers. Although no general conclusions should be made on the incidence of cork taint in the wider wine industry based on the results found within this explorative investigation, these findings confirmed the presence of cork taint in South African wines. Detection threshold values were determined for TCA, TeCA, TBA and PCA in three wine cultivars using the standard ASTM method. Results indicate that factors relating to the wine cultivar seemed to affect threshold values considerably. Our research proposes a detection range rather than an average detection threshold. Detection ranges established for TCA, TeCA, TBA and PCA in Chenin blanc, Pinotage and Shiraz coincide with reported values in literature. This result can be regarded as a valuable expansion of the existing knowledge of detection threshold values. Descriptive sensory analysis indicated significant (P 0.05) changes in the aroma profile of Chenin blanc, Pinotage and Shiraz after TCA, TeCA, TBA or PCA was added to the respective base wines that contained no detectable levels of the haloanisoles. The mouldy taint induced by these haloanisoles were described as mouldy, mouldy-chemical, mouldychlorine, as well as mouldy-acidic. In Chenin blanc, additions of TCA, in the concentration range 1 to 17 ng/L, resulted in a marked increase in the mouldy aroma and was accompanied by an immediate decrease in fruitiness. This change was already evident at added TCA concentrations of 1 ng/L. Similar trends were observed in Pinotage, while the addition of low levels of TCA to Shiraz (2 ng/L) resulted in a significant (P 0.05) decrease in the herbaceous character of the wine. The aroma changes observed were prominent enough to render the wine totally unacceptable in comparison to its original character. Consumers’ degree of liking did not seem to be affected by very low concentration levels of TCA in Chenin blanc, Pinotage or Shiraz, but rejection increased as the concentration increased beyond detection threshold level. A slight gender effect was also noticed. Female consumers appeared to be more sensitive to increasing levels of TCA, whereas male consumers did not respond as negatively to higher concentration levels of TCA. This study makes an important contribution towards understanding the sensory impact of especially TCA contamination in wine, through the establishment of concentration ranges at which these compounds exert a noticeable detrimental effect on the aroma profile of wine. Additional insight into cork taint in wine is provided by the consumer preference studies, where the effects of the taint on the product acceptance by consumers are demonstrated. The development of a modus operandi to ensure that sensory panels provide reliable data, can be regarded as an important contribution to wine-related research. This study is one of the first where advanced sensometric techniques were applied in sensory studies on cork tainted wines. Masters 2009-02-28T10:35:58Z 2010-06-01T08:40:20Z 2009-02-28T10:35:58Z 2010-06-01T08:40:20Z 2009-03 Thesis http://hdl.handle.net/10019.1/2092 en University of Stellenbosch application/pdf Stellenbosch : University of Stellenbosch
spellingShingle Cork taint
Dissertations -- Food science
Theses -- Food science
Bottle corks
Wine -- Flavor and odor -- South Africa
Wine tasting -- South Africa
Van Eeden, Petrus Rabe
Chemical, sensory and consumer analysis of cork taint in South African wines
title Chemical, sensory and consumer analysis of cork taint in South African wines
title_full Chemical, sensory and consumer analysis of cork taint in South African wines
title_fullStr Chemical, sensory and consumer analysis of cork taint in South African wines
title_full_unstemmed Chemical, sensory and consumer analysis of cork taint in South African wines
title_short Chemical, sensory and consumer analysis of cork taint in South African wines
title_sort chemical sensory and consumer analysis of cork taint in south african wines
topic Cork taint
Dissertations -- Food science
Theses -- Food science
Bottle corks
Wine -- Flavor and odor -- South Africa
Wine tasting -- South Africa
url http://hdl.handle.net/10019.1/2092
work_keys_str_mv AT vaneedenpetrusrabe chemicalsensoryandconsumeranalysisofcorktaintinsouthafricanwines